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3'-Nitroacetophenone

CAS# 121-89-1

3'-Nitroacetophenone

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Quality Control of 3'-Nitroacetophenone

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Chemical structure

3'-Nitroacetophenone

3D structure

Chemical Properties of 3'-Nitroacetophenone

Cas No. 121-89-1 SDF Download SDF
PubChem ID 8494 Appearance Cryst.
Formula C8H7NO3 M.Wt 165.15
Type of Compound Miscellaneous Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name 1-(3-nitrophenyl)ethanone
SMILES CC(=O)C1=CC(=CC=C1)[N+](=O)[O-]
Standard InChIKey ARKIFHPFTHVKDT-UHFFFAOYSA-N
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of 3'-Nitroacetophenone

The herbs of Styrax tonkinensis

Protocol of 3'-Nitroacetophenone

Structure Identification
Applied Catalysis A: General, 2013, 462-463:121-128.

Hydrogenation of 3-nitroacetophenone over rhodium/silica catalysts: Effect of metal dispersion and catalyst support[Reference: WebLink]


METHODS AND RESULTS:
The effect of physical properties of rhodium/silica catalysts on the hydrogenation of 3-nitroacetophenone was investigated using a series of catalysts with different particle sizes, pore sizes and dispersions. The hydrogenation reaction was carried out in the liquid phase at different temperatures (313–343 K) and hydrogen pressures (2–5 barg). The hydrogenation of 3-nitroacetophenone was found to be a consecutive reaction with 3-aminoacetophenone, 1-(3-aminophenyl) ethanol, and 1-(3-aminocyclohexyl) ethanol the main products; traces of 3-aminoaniline were also detected. The reaction was zero order with respect to the concentration of 3-nitroacetophenone and half order with respect to hydrogen. The rate of formation and disappearance of intermediates increased with increasing temperature and hydrogen pressure. The rate of ring hydrogenation to form 1-(3-aminocyclohexyl) ethanol shows a marked increase at high temperatures. The catalytic activity varies with both the pore size of silica support and the rhodium dispersion with no significant influence of catalyst particle size. The turnover frequency increases with decreasing metal dispersion (or with increasing average metal crystallite size) revealing an antipathetic particle size effect.
CONCLUSIONS:
This behaviour can be related to changes in the electronic and structural make up of small metal crystallites but suggests that the reaction takes place on the plane face surface of the FCC close-pack structure of rhodium in which the number of face surface atoms increases at the expense of the edge and corner sites as the metal crystallite size increases.

3'-Nitroacetophenone Dilution Calculator

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3'-Nitroacetophenone Molarity Calculator

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Preparing Stock Solutions of 3'-Nitroacetophenone

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 6.0551 mL 30.2755 mL 60.551 mL 121.102 mL 151.3775 mL
5 mM 1.211 mL 6.0551 mL 12.1102 mL 24.2204 mL 30.2755 mL
10 mM 0.6055 mL 3.0276 mL 6.0551 mL 12.1102 mL 15.1378 mL
50 mM 0.1211 mL 0.6055 mL 1.211 mL 2.422 mL 3.0276 mL
100 mM 0.0606 mL 0.3028 mL 0.6055 mL 1.211 mL 1.5138 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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