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Ardisicrenoside B

CAS# 160791-12-8

Ardisicrenoside B

Catalog No. BCN8078----Order now to get a substantial discount!

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Quality Control of Ardisicrenoside B

Number of papers citing our products

Chemical structure

Ardisicrenoside B

3D structure

Chemical Properties of Ardisicrenoside B

Cas No. 160791-12-8 SDF Download SDF
PubChem ID 10373894 Appearance Powder
Formula C52H86O22 M.Wt 1063.23
Type of Compound Triterpenoids Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name (2S,3R,4S,5S,6R)-2-[(2S,3R,4S,5S)-5-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4S,5R)-3,4,5-trihydroxyoxan-2-yl]oxyoxan-2-yl]oxy-4-hydroxy-2-[[(1S,2R,4S,5R,8R,10S,13R,14R,17S,18R,20S)-2-hydroxy-20-(hydroxymethyl)-4,5,9,9,13,20-hexamethyl-24-oxahexacyclo[15.5.2.01,18.04,17.05,14.08,13]tetracosan-10-yl]oxy]oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol
SMILES CC1(C2CCC3(C(C2(CCC1OC4C(C(C(CO4)OC5C(C(C(C(O5)CO)O)O)OC6C(C(C(CO6)O)O)O)O)OC7C(C(C(C(O7)CO)O)O)O)C)CCC89C3(CC(C1(C8CC(CC1)(C)CO)CO9)O)C)C)C
Standard InChIKey RDBUKNALARTFFW-VKKSEJOZSA-N
Standard InChI InChI=1S/C52H86O22/c1-46(2)27-7-11-49(5)28(8-12-52-29-15-47(3,21-55)13-14-51(29,22-68-52)30(57)16-50(49,52)6)48(27,4)10-9-31(46)72-44-40(74-43-39(65)36(62)33(59)24(17-53)69-43)35(61)26(20-67-44)71-45-41(37(63)34(60)25(18-54)70-45)73-42-38(64)32(58)23(56)19-66-42/h23-45,53-65H,7-22H2,1-6H3/t23-,24-,25-,26+,27+,28-,29-,30-,31+,32+,33-,34-,35+,36+,37+,38-,39-,40-,41-,42+,43+,44+,45+,47+,48+,49-,50+,51-,52+/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of Ardisicrenoside B

The herbs of Ardisia crenata

Biological Activity of Ardisicrenoside B

In vitro

Quantitative determination of triperpene saponins and alkenated-phenolics from Labisia pumila using an LC-UV/ELSD method and confirmation by LC-ESI-TOF.[Pubmed: 21590653 ]

Planta Med. 2011 Oct;77(15):1742-8.

This study describes the first analytical method for the determination of four triterpene saponins (Ardisicrenoside B, ardisiacrispin A, 3- O- α- L-rhamnopyranosyl-(1 → 2)-β-D-glucopyranosyl-(1 → 4)-α-L-arabinopynanosyl cyclamiretin A and ardisimamilloside H) and three alkenated-phenolics (irisresorcinol, belamcandol B, and demethylbelamcandaquinone B) from the leaves, leaves/stems, and roots of LABISIA PUMILA using an HPLC-UV-ELSD method.
METHODS AND RESULTS:
The separation was achieved using a reversed-phase (C-18) column, PDA and ELS detection, and a water/acetonitrile gradient as the mobile phase. The major triterpenoid (ardisiacrispin A) and irisresorcinol compounds were detected at a concentration as low as 10.0 and 0.2 μg/mL, respectively. Analysis of various samples showed considerable variation of 0.11-2.46 % for the major triterpenoid compound, ardisiacrispin A. LC-mass spectrometry method coupled with electrospray ionization (ESI) is described for the identification of compounds in plant samples.
CONCLUSIONS:
This method involved the use of the [M + Na]+ and [M + NH₄]+ ions for compounds 1-4 in the positive ion mode with extractive ion chromatogram (EIC).

Protocol of Ardisicrenoside B

Structure Identification
J Asian Nat Prod Res. 2008 Mar-Apr;10(3-4):291-6.

Triterpene saponins from Lysimachia christinae.[Pubmed: 18335347 ]


METHODS AND RESULTS:
Seven triterpene saponins were isolated from Lysimachia christinae and identified as lysichriside A (1), lysichriside B (2), primulanin (3), lysikokianoside 1 (4), anagallisin C (5), ardisiacrispin A (6), and Ardisicrenoside B (7). Compounds 1 and 2 are new triterpene saponins, compounds 3, 5, and 7 were isolated from this genus, and compounds 4 and 6 were isolated from this species for the first time.
CONCLUSIONS:
Their structures were elucidated by means of 1D and 2D NMR experiments.

Ardisicrenoside B Dilution Calculator

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Ardisicrenoside B Molarity Calculator

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Preparing Stock Solutions of Ardisicrenoside B

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 0.9405 mL 4.7027 mL 9.4053 mL 18.8106 mL 23.5133 mL
5 mM 0.1881 mL 0.9405 mL 1.8811 mL 3.7621 mL 4.7027 mL
10 mM 0.0941 mL 0.4703 mL 0.9405 mL 1.8811 mL 2.3513 mL
50 mM 0.0188 mL 0.0941 mL 0.1881 mL 0.3762 mL 0.4703 mL
100 mM 0.0094 mL 0.047 mL 0.0941 mL 0.1881 mL 0.2351 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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References on Ardisicrenoside B

Quantitative determination of triperpene saponins and alkenated-phenolics from Labisia pumila using an LC-UV/ELSD method and confirmation by LC-ESI-TOF.[Pubmed:21590653]

Planta Med. 2011 Oct;77(15):1742-8.

This study describes the first analytical method for the determination of four triterpene saponins (Ardisicrenoside B, ardisiacrispin A, 3- O- alpha- L-rhamnopyranosyl-(1 --> 2)-beta-D-glucopyranosyl-(1 --> 4)-alpha-L-arabinopynanosyl cyclamiretin A and ardisimamilloside H) and three alkenated-phenolics (irisresorcinol, belamcandol B, and demethylbelamcandaquinone B) from the leaves, leaves/stems, and roots of LABISIA PUMILA using an HPLC-UV-ELSD method. The separation was achieved using a reversed-phase (C-18) column, PDA and ELS detection, and a water/acetonitrile gradient as the mobile phase. The major triterpenoid (ardisiacrispin A) and irisresorcinol compounds were detected at a concentration as low as 10.0 and 0.2 microg/mL, respectively. Analysis of various samples showed considerable variation of 0.11-2.46 % for the major triterpenoid compound, ardisiacrispin A. LC-mass spectrometry method coupled with electrospray ionization (ESI) is described for the identification of compounds in plant samples. This method involved the use of the [M + Na]+ and [M + NH(4)]+ ions for compounds 1-4 in the positive ion mode with extractive ion chromatogram (EIC).

Triterpene saponins from Lysimachia christinae.[Pubmed:18335347]

J Asian Nat Prod Res. 2008 Mar-Apr;10(3-4):291-6.

Seven triterpene saponins were isolated from Lysimachia christinae and identified as lysichriside A (1), lysichriside B (2), primulanin (3), lysikokianoside 1 (4), anagallisin C (5), ardisiacrispin A (6), and Ardisicrenoside B (7). Compounds 1 and 2 are new triterpene saponins, compounds 3, 5, and 7 were isolated from this genus, and compounds 4 and 6 were isolated from this species for the first time. Their structures were elucidated by means of 1D and 2D NMR experiments.

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