Rheum hotaoense
Rheum hotaoense
1. The products in our compound library are selected from thousands of unique natural products; 2. It has the characteristics of diverse structure, diverse sources and wide coverage of activities; 3. Provide information on the activity of products from major journals, patents and research reports around the world, providing theoretical direction and research basis for further research and screening; 4. Free combination according to the type, source, target and disease of natural product; 5. The compound powder is placed in a covered tube and then discharged into a 10 x 10 cryostat; 6. Transport in ice pack or dry ice pack. Please store it at -20 °C as soon as possible after receiving the product, and use it as soon as possible after opening.
Natural products/compounds from Rheum hotaoense
- Cat.No. Product Name CAS Number COA
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BCN5392
Rhaponiticin155-58-8
Instructions
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BCN3515
Rhapontigenin500-65-2
Instructions
Two-dimensional preparative liquid chromatography system for preparative separation of minor amount components from complicated natural products.[Pubmed: 24745752]
An on-line comprehensive two-dimensional preparative liquid chromatography system was developed for preparative separation of minor amount components from complicated natural products. Medium-pressure liquid chromatograph (MPLC) was applied as the first dimension and preparative HPLC as the second one, in conjunction with trapping column and makeup pump. The performance of the trapping column was evaluated, in terms of column size, dilution ratio and diameter-height ratio, as well as system pressure from the view of medium pressure liquid chromatograph. Satisfactory trapping efficiency can be achieved using a commercially available 15 mm × 30 mm i.d. ODS pre-column. The instrument operation and the performance of this MPLC×preparative HPLC system were illustrated by gram-scale isolation of crude macro-porous resin enriched water extract of Rheum hotaoense. Automated multi-step preparative separation of 25 compounds, whose structures were identified by MS, (1)H NMR and even by less-sensitive (13)C NMR, could be achieved in a short period of time using this system, exhibiting great advantages in analytical efficiency and sample treatment capacity compared with conventional methods.
[Quantitative determination of rhapontin in root of Rheum hotaoense by TLC-scanning].[Pubmed: 8011123]
The contents of rhapontin in the root of Rheum hotaoense were determined by CS-920 TLC-scanning of silica gel plate A mixture of benzene-EtOAc-EtOH (5 : 3, 5 : 1.5) was used as the developing solvent. Recovery was 100.44%, RSD 3.0%.
