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Paniculidine B

CAS# 97399-94-5

Paniculidine B

Catalog No. BCN4523----Order now to get a substantial discount!

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Quality Control of Paniculidine B

Number of papers citing our products

Chemical structure

Paniculidine B

3D structure

Chemical Properties of Paniculidine B

Cas No. 97399-94-5 SDF Download SDF
PubChem ID 14070748 Appearance Oil
Formula C14H19NO2 M.Wt 233.3
Type of Compound Alkaloids Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name (2R)-4-(1-methoxyindol-3-yl)-2-methylbutan-1-ol
SMILES CC(CCC1=CN(C2=CC=CC=C21)OC)CO
Standard InChIKey FGYVMFMFZWJGDY-LLVKDONJSA-N
Standard InChI InChI=1S/C14H19NO2/c1-11(10-16)7-8-12-9-15(17-2)14-6-4-3-5-13(12)14/h3-6,9,11,16H,7-8,10H2,1-2H3/t11-/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of Paniculidine B

The herbs of Murraya exotica L.

Biological Activity of Paniculidine B

DescriptionStandard reference

Protocol of Paniculidine B

Structure Identification
J Org Chem. 2004 Jun 25;69(13):4429-32.

Efficient total syntheses of phytoalexin and (+/-)-paniculidine B and C based on the novel methodology for the preparation of 1-methoxyindoles.[Pubmed: 15202897]


METHODS AND RESULTS:
A general route to 2-unsubstituted-1-methoxyindoles, based on our methodology for the synthesis of 1-methoxyindoles, is reported. This synthesis renders accessibility to a variety of natural products possessing the said skeleton. A direct synthesis of phytoalexin (1), (+/-)-Paniculidine B (2), and (+/-)-paniculidine C (3) is disclosed based on the methodology.
CONCLUSIONS:
The synthesis of Paniculidine B (2) has been achieved from aldehyde 10 in only two steps in 88% yield and in five steps from a methoxyindole compound 8 obtained using our earlier methodology.

Chemical & Pharmaceutical Bulletin , 1985 , 33 (4) :1770-3

Structures of paniculidines A and B: novel prenylindoles from Murraya paniculata[Reference: WebLink]


METHODS AND RESULTS:
Two new indoles named Paniculidine A and Paniculidine B were isolated from Murraya paniculata (Linn.) Jack., and their structures have been elucidated as methyl 2-methyl-4-(indol-3-yl)-butyrate and 2-methyl-4-(1-methoxyindol-3-yl)-1-butanol, respectively.

Paniculidine B Dilution Calculator

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Paniculidine B Molarity Calculator

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Preparing Stock Solutions of Paniculidine B

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 4.2863 mL 21.4316 mL 42.8633 mL 85.7265 mL 107.1582 mL
5 mM 0.8573 mL 4.2863 mL 8.5727 mL 17.1453 mL 21.4316 mL
10 mM 0.4286 mL 2.1432 mL 4.2863 mL 8.5727 mL 10.7158 mL
50 mM 0.0857 mL 0.4286 mL 0.8573 mL 1.7145 mL 2.1432 mL
100 mM 0.0429 mL 0.2143 mL 0.4286 mL 0.8573 mL 1.0716 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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References on Paniculidine B

Efficient total syntheses of phytoalexin and (+/-)-paniculidine B and C based on the novel methodology for the preparation of 1-methoxyindoles.[Pubmed:15202897]

J Org Chem. 2004 Jun 25;69(13):4429-32.

A general route to 2-unsubstituted-1-methoxyindoles, based on our methodology for the synthesis of 1-methoxyindoles, is reported. This synthesis renders accessibility to a variety of natural products possessing the said skeleton. A direct synthesis of phytoalexin (1), (+/-)-Paniculidine B (2), and (+/-)-paniculidine C (3) is disclosed based on the methodology. The synthesis of Paniculidine B (2) has been achieved from aldehyde 10 in only two steps in 88% yield and in five steps from a methoxyindole compound 8 obtained using our earlier methodology.

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