3H-1,2-Benzodithiol-3-one-1,1-dioxideCAS# 66304-01-6 |
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| Cas No. | 66304-01-6 | SDF | Download SDF |
| PubChem ID | 3009847 | Appearance | Powder |
| Formula | C7H4O3S2 | M.Wt | 200 |
| Type of Compound | N/A | Storage | Desiccate at -20°C |
| Solubility | DMSO : ≥ 100 mg/mL (499.43 mM) H2O : < 0.1 mg/mL (insoluble) *"≥" means soluble, but saturation unknown. | ||
| Chemical Name | 1,1-dioxo-1$l^{6},2-benzodithiol-3-one | ||
| SMILES | C1=CC=C2C(=C1)C(=O)SS2(=O)=O | ||
| Standard InChIKey | JUDOLRSMWHVKGX-UHFFFAOYSA-N | ||
| Standard InChI | InChI=1S/C7H4O3S2/c8-7-5-3-1-2-4-6(5)12(9,10)11-7/h1-4H | ||
| General tips | For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months. We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months. Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it. |
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| About Packaging | 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial. 2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial. 3. Try to avoid loss or contamination during the experiment. |
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| Shipping Condition | Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request. | ||
3H-1,2-Benzodithiol-3-one-1,1-dioxide Dilution Calculator
3H-1,2-Benzodithiol-3-one-1,1-dioxide Molarity Calculator
| 1 mg | 5 mg | 10 mg | 20 mg | 25 mg | |
| 1 mM | 5 mL | 25 mL | 50 mL | 100 mL | 125 mL |
| 5 mM | 1 mL | 5 mL | 10 mL | 20 mL | 25 mL |
| 10 mM | 0.5 mL | 2.5 mL | 5 mL | 10 mL | 12.5 mL |
| 50 mM | 0.1 mL | 0.5 mL | 1 mL | 2 mL | 2.5 mL |
| 100 mM | 0.05 mL | 0.25 mL | 0.5 mL | 1 mL | 1.25 mL |
| * Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations. | |||||
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Solid-phase chemical synthesis of phosphonoacetate and thiophosphonoacetate oligodeoxynucleotides.[Pubmed:12537492]
J Am Chem Soc. 2003 Jan 29;125(4):940-50.
Phosphonoacetate and thiophosphonoacetate oligodeoxynucleotides were prepared via a solid-phase synthesis strategy. Under Reformatsky reaction conditions, novel esterified acetic acid phosphinodiamidites were synthesized and condensed with appropriately protected 5'-O-(4, 4'-dimethoxytrityl)-2'-deoxynucleosides to yield 3'-O-phosphinoamidite reactive monomers. These synthons when activated with tetrazole were used with an automated DNA synthesizer to prepare phosphonoacetic acid modified internucleotide linkages on controlled pore glass. The phosphinoacetate coupling products were quantitatively oxidized at each step with (1S)-(+)-(10-camphorsulfonyl)oxaziridine or 3H-1,2-Benzodithiol-3-one-1,1-dioxide to produce mixed sequence phosphonoacetate and thiophosphonoacetate oligodeoxynucleotides with an average per cycle coupling efficiency of greater than 97%. Completely deprotected, modified oligodeoxynucleotides were purified by reverse-phase HPLC and characterized by ion exchange HPLC, (31)P NMR, and MALDI/TOF mass spectroscopy. Both analogues were stable toward hydrolysis with snake venom phosphodiesterase and stimulated RNase H1 activity.
Beaucage reagent is found to be potent in causing DNA cleavage.
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