H-Val-OtBu.HClCAS# 13518-40-6 |
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| Cas No. | 13518-40-6 | SDF | Download SDF |
| PubChem ID | 12490702 | Appearance | Powder |
| Formula | C9H20ClNO2 | M.Wt | 209.7 |
| Type of Compound | N/A | Storage | Desiccate at -20°C |
| Solubility | Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc. | ||
| Chemical Name | tert-butyl (2S)-2-amino-3-methylbutanoate;hydrochloride | ||
| SMILES | CC(C)C(C(=O)OC(C)(C)C)N.Cl | ||
| Standard InChIKey | AUIVQIHTTVPKFS-FJXQXJEOSA-N | ||
| Standard InChI | InChI=1S/C9H19NO2.ClH/c1-6(2)7(10)8(11)12-9(3,4)5;/h6-7H,10H2,1-5H3;1H/t7-;/m0./s1 | ||
| General tips | For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months. We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months. Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it. |
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| About Packaging | 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial. 2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial. 3. Try to avoid loss or contamination during the experiment. |
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| Shipping Condition | Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request. | ||
H-Val-OtBu.HCl Dilution Calculator
H-Val-OtBu.HCl Molarity Calculator
| 1 mg | 5 mg | 10 mg | 20 mg | 25 mg | |
| 1 mM | 4.7687 mL | 23.8436 mL | 47.6872 mL | 95.3743 mL | 119.2179 mL |
| 5 mM | 0.9537 mL | 4.7687 mL | 9.5374 mL | 19.0749 mL | 23.8436 mL |
| 10 mM | 0.4769 mL | 2.3844 mL | 4.7687 mL | 9.5374 mL | 11.9218 mL |
| 50 mM | 0.0954 mL | 0.4769 mL | 0.9537 mL | 1.9075 mL | 2.3844 mL |
| 100 mM | 0.0477 mL | 0.2384 mL | 0.4769 mL | 0.9537 mL | 1.1922 mL |
| * Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations. | |||||
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H-Val-OtBu•HCl
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Stereocontrolled synthesis of psi[CH(CF3)NH]gly-peptides.[Pubmed:14535735]
Org Lett. 2003 Oct 16;5(21):3887-90.
[reaction: see text] A novel class of peptidomimetics having a stereogenic [CH(CF(3))NH] replacement for a [CONH] peptide bond has been synthesized. The new compounds have been obtained in a stereocontrolled fashion using a kinetically controlled aza-Michael addition of chiral alpha-amino acid esters to trans-3,3,3-trifluoro-1-nitropropene. The stereoselectivity is strongly influenced by the solvent, the base, its stoichiometry, and the R side-chain. Diastereomeric ratios higher than 11:1 were achieved using H-Val-OtBu.HCl in toluene with 1.1 equiv of DIPEA.
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