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(-)-Lyoniresinol 9'-O-glucoside

CAS# 143236-02-6

(-)-Lyoniresinol 9'-O-glucoside

Catalog No. BCN7037----Order now to get a substantial discount!

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(-)-Lyoniresinol 9'-O-glucoside: 5mg $828 In Stock
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Quality Control of (-)-Lyoniresinol 9'-O-glucoside

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Chemical structure

(-)-Lyoniresinol 9'-O-glucoside

3D structure

Chemical Properties of (-)-Lyoniresinol 9'-O-glucoside

Cas No. 143236-02-6 SDF Download SDF
PubChem ID 10031185 Appearance Powder
Formula C28H38O13 M.Wt 582.59
Type of Compound Lignans Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name (2R,3R,4S,5S,6R)-2-[[(1R,2S,3S)-7-hydroxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-3-(hydroxymethyl)-6,8-dimethoxy-1,2,3,4-tetrahydronaphthalen-2-yl]methoxy]-6-(hydroxymethyl)oxane-3,4,5-triol
SMILES COC1=CC(=CC(=C1O)OC)C2C(C(CC3=CC(=C(C(=C23)OC)O)OC)CO)COC4C(C(C(C(O4)CO)O)O)O
Standard InChIKey PQQRNPDHSJDAGV-UGJKOEBBSA-N
Standard InChI InChI=1S/C28H38O13/c1-36-16-7-13(8-17(37-2)22(16)31)20-15(11-40-28-26(35)25(34)23(32)19(10-30)41-28)14(9-29)5-12-6-18(38-3)24(33)27(39-4)21(12)20/h6-8,14-15,19-20,23,25-26,28-35H,5,9-11H2,1-4H3/t14-,15-,19-,20+,23-,25+,26-,28-/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of (-)-Lyoniresinol 9'-O-glucoside

The bamboo-sheath of Phyllostachys heterocycla MITF.

Biological Activity of (-)-Lyoniresinol 9'-O-glucoside

Description(-)-Lyoniresinol 9'-O-glucoside is a natural product from Phyllostachys heterocycla MITF.

Protocol of (-)-Lyoniresinol 9'-O-glucoside

Structure Identification
Chem Pharm Bull (Tokyo). 2017;65(9):878-882.

Identification of Characteristic Phenolic Constituents in Mousouchiku Extract Used as Food Additives.[Pubmed: 28867716 ]

Mousouchiku extract is prepared from the bamboo-sheath of Phyllostachys heterocycla MITF. (Poaceae), and is registered as a food manufacturing agent in the List of Existing Food Additives in Japan.
METHODS AND RESULTS:
This study describes the chromatographic evaluation of characteristic components of this extract to obtain the chemical data needed for standardized specifications. We isolated 12 known compounds from this extract: 5-hydroxymethyl-2-furfural, 4-hydroxybenzoic acid, trans-p-coumaric acid, trans-ferulic acid, N,N'-diferuloylputrescine, 4'-hydroxypropiophenone, β-arbutin, tachioside, isotachioside, 3,4'-dihydroxypropiophenone 3-O-glucoside, koaburaside, and (+)-lyoniresinol 9'-O-glucoside. Moreover, a new propiophenone glycoside, propiophenone 4'-O-(6-β-D-xylosyl)-β-D-glucoside (propiophenone 4'-O-primeveroside), was isolated. The structure of each isolated compound was elucidated based on NMR and MS data or direct HPLC comparisons with authentic samples.
CONCLUSIONS:
Among the isolates, (+)-lyoniresinol 9'-O-glucoside was found to be the major ingredients of the extract as observed using HPLC analysis. However, 2,6-dimethoxy-1,4-benzoquinone, which is considered the main constituent of mousouchiku extract, was only detected as a trace constituent and not isolated in this study.

(-)-Lyoniresinol 9'-O-glucoside Dilution Calculator

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(-)-Lyoniresinol 9'-O-glucoside Molarity Calculator

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Preparing Stock Solutions of (-)-Lyoniresinol 9'-O-glucoside

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 1.7165 mL 8.5824 mL 17.1647 mL 34.3295 mL 42.9118 mL
5 mM 0.3433 mL 1.7165 mL 3.4329 mL 6.8659 mL 8.5824 mL
10 mM 0.1716 mL 0.8582 mL 1.7165 mL 3.4329 mL 4.2912 mL
50 mM 0.0343 mL 0.1716 mL 0.3433 mL 0.6866 mL 0.8582 mL
100 mM 0.0172 mL 0.0858 mL 0.1716 mL 0.3433 mL 0.4291 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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References on (-)-Lyoniresinol 9'-O-glucoside

Identification of Characteristic Phenolic Constituents in Mousouchiku Extract Used as Food Additives.[Pubmed:28867716]

Chem Pharm Bull (Tokyo). 2017;65(9):878-882.

Mousouchiku extract is prepared from the bamboo-sheath of Phyllostachys heterocycla MITF. (Poaceae), and is registered as a food manufacturing agent in the List of Existing Food Additives in Japan. This study describes the chromatographic evaluation of characteristic components of this extract to obtain the chemical data needed for standardized specifications. We isolated 12 known compounds from this extract: 5-hydroxymethyl-2-furfural, 4-hydroxybenzoic acid, trans-p-coumaric acid, trans-ferulic acid, N,N'-diferuloylputrescine, 4'-hydroxypropiophenone, beta-arbutin, tachioside, isotachioside, 3,4'-dihydroxypropiophenone 3-O-glucoside, koaburaside, and (+)-lyoniresinol 9'-O-glucoside. Moreover, a new propiophenone glycoside, propiophenone 4'-O-(6-beta-D-xylosyl)-beta-D-glucoside (propiophenone 4'-O-primeveroside), was isolated. The structure of each isolated compound was elucidated based on NMR and MS data or direct HPLC comparisons with authentic samples. Among the isolates, (+)-lyoniresinol 9'-O-glucoside was found to be the major ingredients of the extract as observed using HPLC analysis. However, 2,6-dimethoxy-1,4-benzoquinone, which is considered the main constituent of mousouchiku extract, was only detected as a trace constituent and not isolated in this study.

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