Hythiemoside BCAS# 853267-90-0 |
Quality Control & MSDS
Number of papers citing our products
Chemical structure
3D structure
Cas No. | 853267-90-0 | SDF | Download SDF |
PubChem ID | 11203296 | Appearance | Powder |
Formula | C28H46O9 | M.Wt | 526.7 |
Type of Compound | Diterpenoids | Storage | Desiccate at -20°C |
Solubility | Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc. | ||
Chemical Name | [(1R)-1-[(2S,4aR,4bS,7R,8aS)-2,4b,8,8-tetramethyl-7-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-4,4a,5,6,7,8a,9,10-octahydro-3H-phenanthren-2-yl]-2-hydroxyethyl] acetate | ||
SMILES | CC(=O)OC(CO)C1(CCC2C(=C1)CCC3C2(CCC(C3(C)C)OC4C(C(C(C(O4)CO)O)O)O)C)C | ||
Standard InChIKey | POOFTLXTGZSZGA-AUNXJCHXSA-N | ||
Standard InChI | InChI=1S/C28H46O9/c1-15(31)35-21(14-30)27(4)10-8-17-16(12-27)6-7-19-26(2,3)20(9-11-28(17,19)5)37-25-24(34)23(33)22(32)18(13-29)36-25/h12,17-25,29-30,32-34H,6-11,13-14H2,1-5H3/t17-,18-,19-,20-,21+,22-,23+,24-,25+,27+,28+/m1/s1 | ||
General tips | For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months. We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months. Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it. |
||
About Packaging | 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial. 2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial. 3. Try to avoid loss or contamination during the experiment. |
||
Shipping Condition | Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request. |
Structure Identification | Chem Pharm Bull (Tokyo). 2005 Feb;53(2):232-4.ent-pimarane-type diterpenoids from Siegesbeckia orientalis L.[Pubmed: 15684525 ]
|
Hythiemoside B Dilution Calculator
Hythiemoside B Molarity Calculator
1 mg | 5 mg | 10 mg | 20 mg | 25 mg | |
1 mM | 1.8986 mL | 9.4931 mL | 18.9861 mL | 37.9723 mL | 47.4654 mL |
5 mM | 0.3797 mL | 1.8986 mL | 3.7972 mL | 7.5945 mL | 9.4931 mL |
10 mM | 0.1899 mL | 0.9493 mL | 1.8986 mL | 3.7972 mL | 4.7465 mL |
50 mM | 0.038 mL | 0.1899 mL | 0.3797 mL | 0.7594 mL | 0.9493 mL |
100 mM | 0.019 mL | 0.0949 mL | 0.1899 mL | 0.3797 mL | 0.4747 mL |
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations. |
Calcutta University
University of Minnesota
University of Maryland School of Medicine
University of Illinois at Chicago
The Ohio State University
University of Zurich
Harvard University
Colorado State University
Auburn University
Yale University
Worcester Polytechnic Institute
Washington State University
Stanford University
University of Leipzig
Universidade da Beira Interior
The Institute of Cancer Research
Heidelberg University
University of Amsterdam
University of Auckland
TsingHua University
The University of Michigan
Miami University
DRURY University
Jilin University
Fudan University
Wuhan University
Sun Yat-sen University
Universite de Paris
Deemed University
Auckland University
The University of Tokyo
Korea University
- Randialic acid B
Catalog No.:BCN8832
CAS No.:14021-14-8
- Harmidol hydrochloride
Catalog No.:BCN8831
CAS No.:6028-07-5
- Cassiaside B2
Catalog No.:BCN8830
CAS No.:218155-40-9
- Anemarrhenasaponin III
Catalog No.:BCN8829
CAS No.:163047-23-2
- Isorhamnetin 3,7-O-diglucoside
Catalog No.:BCN8828
CAS No.:6758-51-6
- 5'''-O-Feruloyl complanatoside B
Catalog No.:BCN8827
CAS No.:142473-98-1
- 11-Oxomogroside IV
Catalog No.:BCN8826
CAS No.:2096516-32-2
- Chrysophanol 1-O-beta-tetraglucoside
Catalog No.:BCN8825
CAS No.:120181-08-0
- Ardisicrenoside A
Catalog No.:BCN8824
CAS No.:160824-52-2
- Ardisiacrispin B
Catalog No.:BCN8823
CAS No.:112766-96-8
- Combretol
Catalog No.:BCN8822
CAS No.:5084-19-5
- 5,7,3',4'-Tetramethoxyflavone
Catalog No.:BCN8821
CAS No.:855-97-0
- Notoginsenoside R4
Catalog No.:BCN8834
CAS No.:87741-77-3
- 4H-1-Benzopyran-4-one,2,3-dihydro-5-hydroxy-3-[(4-hydroxyphenyl)methyl]-7-methoxy-
Catalog No.:BCN8835
CAS No.:108001-32-7
- 6-Hydroxykaempferol 3-O-beta-D-glucoside
Catalog No.:BCN8836
CAS No.:145134-61-8
- Quercetin 3-O-neohesperidoside
Catalog No.:BCN8837
CAS No.:32453-36-4
- Arjunetin
Catalog No.:BCN8838
CAS No.:31297-79-7
- Celosin J
Catalog No.:BCN8839
CAS No.:1623405-29-7
- Iso-sagittatoside A
Catalog No.:BCN8840
CAS No.:503456-08-4
- Hydroxy-beta-sanshool
Catalog No.:BCN8841
CAS No.:97465-69-5
- Mulberrofuran Q
Catalog No.:BCN8844
CAS No.:101383-35-1
- 4'-Methoxyagarotetrol
Catalog No.:BCN8845
CAS No.:123278-01-3
- Sterebin E
Catalog No.:BCN8846
CAS No.:114343-74-7
- Bacopaside N2
Catalog No.:BCN8847
CAS No.:871706-75-1
Simultaneous determination of seven major diterpenoids in Siegesbeckia pubescens Makino by high-performance liquid chromatography coupled with evaporative light scattering detection.[Pubmed:22887919]
J Sep Sci. 2012 Oct;35(19):2585-91.
A novel HPLC method with evaporative light scattering detection was developed for the simultaneous quantification of seven major diterpenoids of two types, including ent-pimarane type: Kirenol, Hythiemoside B, Darutigenol, and ent-kaurane type: ent-16beta,17,18-trihydroxy-kauran-19-oic acid, ent-17,18-dihydroxy-kauran-19-oic acid, ent-16beta,17-dihydroxy-kauran-19-oic acid, 16alpha-hydro-ent-kauran-17,19-dioic acid in the aerial parts of Siegesbeckia pubescens Makino, an important traditional Chinese medicinal herb. Chromatographic separation was achieved on a Waters Symmetry Shield(TM) RP18 column (250 mmx 4.6 mm id, 5 mum) with a gradient mobile phase (A: 0.3% v/v aqueous formic acid and B: acetonitrile) at a flow rate of 1.0 mL/min. The drift tube temperature of evaporative light scattering detection was set at 103 degrees C, and nitrogen flow rate was 3.0 L/min. The method was validated for accuracy, precision, LOD, and LOQ. All calibration curves showed a good linear relationship (r > 0.999) in test range. Precision was evaluated by intra- and interday tests that showed RSDs were less than 3.5%. Accuracy validation showed that the recovery was between 96.5 and 102.0% with RSDs below 2.8%. The validated method was successfully applied to determine the contents of seven diterpenoids in the different parts of Siegesbeckia pubescens Makino from two sources and to determine the contents of ent-pimarane, ent-kaurane, and total diterpenoids.
ent-pimarane-type diterpenoids from Siegesbeckia orientalis L.[Pubmed:15684525]
Chem Pharm Bull (Tokyo). 2005 Feb;53(2):232-4.
A new ent-pimarane glucoside, named Hythiemoside B (4), was isolated from the aerial part of Siegesbecikia orientalis L. (Asteraceae) together with four known ent-pimarane-type diterpenoids: darutigenol (1), darutoside (2), hythiemoside A (3), and ent-(15R),16,19-trihydroxypimar-8(14)-ene 19-O-beta-D-glucopyranoside (5). The structure of the new compound was elucidated by spectroscopic analyses and chemical transformation. The NMR data of compounds 1 (1H-) and 5 (1H- and 13C-) were also compiled in this study on the basis of 2D experiments.