Shikonofuran A

CAS# 85022-66-8

Shikonofuran A

Catalog No. BCN2826----Order now to get a substantial discount!

Product Name & Size Price Stock
Shikonofuran A: 5mg $667 In Stock
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Quality Control of Shikonofuran A

Number of papers citing our products

Chemical structure

Shikonofuran A

3D structure

Chemical Properties of Shikonofuran A

Cas No. 85022-66-8 SDF Download SDF
PubChem ID 5321286 Appearance Powder
Formula C18H20O5 M.Wt 316.35
Type of Compound Miscellaneous Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name [1-[5-(2,5-dihydroxyphenyl)furan-3-yl]-4-methylpent-3-enyl] acetate
SMILES CC(=CCC(C1=COC(=C1)C2=C(C=CC(=C2)O)O)OC(=O)C)C
Standard InChIKey IMZVJDUASUPZQK-UHFFFAOYSA-N
Standard InChI InChI=1S/C18H20O5/c1-11(2)4-7-17(23-12(3)19)13-8-18(22-10-13)15-9-14(20)5-6-16(15)21/h4-6,8-10,17,20-21H,7H2,1-3H3
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of Shikonofuran A

The roots of Lithosperraum erythrorhizon Sieb. et Zucc.

Protocol of Shikonofuran A

Structure Identification
Chemical and Pharmaceutical Bulletin (Tokyo)1982 30(12): 4407-4411

Shikon 3. new furyl hydro quinone derivatives shikono furans a b c d and e from lithospermum erythrorhizon[Reference: WebLink]


METHODS AND RESULTS:
Five new furylhydroquinone derivatives, named shikonofurans A, B, C, D and E, were found in the root of Lithospermum erythrorhizon (Boraginaceae). Shikonofuran A had the structure I, shown in chart 1, by direct comparison of the spectral data of its diacetate with those of echinofuran leucoacetate. The structures of the other compounds were established on the basis of spectral and chemical evidence as II [B], III [C], IV [D] and V [E], shown in chart 1.

Shikonofuran A Dilution Calculator

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Shikonofuran A Molarity Calculator

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Preparing Stock Solutions of Shikonofuran A

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 3.1611 mL 15.8053 mL 31.6106 mL 63.2211 mL 79.0264 mL
5 mM 0.6322 mL 3.1611 mL 6.3221 mL 12.6442 mL 15.8053 mL
10 mM 0.3161 mL 1.5805 mL 3.1611 mL 6.3221 mL 7.9026 mL
50 mM 0.0632 mL 0.3161 mL 0.6322 mL 1.2644 mL 1.5805 mL
100 mM 0.0316 mL 0.1581 mL 0.3161 mL 0.6322 mL 0.7903 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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References on Shikonofuran A

Systematic identification of shikonins and shikonofurans in medicinal Zicao species using ultra-high performance liquid chromatography quadrupole time of flight tandem mass spectrometry combined with a data mining strategy.[Pubmed:26610615]

J Chromatogr A. 2015 Dec 18;1425:158-72.

Shikonin, Shikonofuran And their derivatives are the main bioactive components of Zicao, a traditional Chinese herbal medicine prepared with the dried roots of Lithospermum erythrorhizon, Arnebia euchroma or Arnebia guttata. However, approaches on the systematic discovery and identification of shikonins and shikonofurans, especially unknown ones, are still not available. To address this issue, the gas-phase CID-fragmentation routes for the shikonins and shikonofurans were established by using ESI-QTOF-MS in the negative ion mode and low-energy collision induced dissociation tandem mass spectrometry (CID-MS/MS) in this study using seventeen standards. As a result, diagnostic product ions for rapid discovery and classification of shikonins and shikonofurans were determined. In addition, various mobile phase compositions and UHPLC elution programs were evaluated to achieve optimal separation efficiency and detection response of these types of analytes. Based on these findings, an integral approach using UHPLC-ESI-QTOF-MS and CID-MS/MS analyses together with a novel two steps data mining strategy was developed for systematic analysis of shikonins and shikonofurans in complex samples. Consequently, 58 compounds including 32 novel ones were efficiently discovered and identified from the crude extract of Zicao. Moreover, comparative analyses of the 58 chemical components in three Zicao species including Lithospermum erythrorhizon, Arnebia euchroma and Arnebia guttata samples were conducted using the established analytical method, which can be instructive for future utilization of Zicao and its related medicinal products.

Description

Shikonofuran A is a natural product isolated from the root of Lithosperraum erythrorhizon Sieb.

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