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1-O-galloyl-6-O-cinnamoylglucose

CAS# 115746-69-5

1-O-galloyl-6-O-cinnamoylglucose

Catalog No. BCN8264----Order now to get a substantial discount!

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1-O-galloyl-6-O-cinnamoylglucose: 5mg $380 In Stock
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Quality Control of 1-O-galloyl-6-O-cinnamoylglucose

Number of papers citing our products

Chemical structure

1-O-galloyl-6-O-cinnamoylglucose

3D structure

Chemical Properties of 1-O-galloyl-6-O-cinnamoylglucose

Cas No. 115746-69-5 SDF Download SDF
PubChem ID 14034234 Appearance Powder
Formula C22H22O11 M.Wt 462.4
Type of Compound Phenols Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name [(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-[[(E)-3-phenylprop-2-enoyl]oxymethyl]oxan-2-yl] 3,4,5-trihydroxybenzoate
SMILES C1=CC=C(C=C1)C=CC(=O)OCC2C(C(C(C(O2)OC(=O)C3=CC(=C(C(=C3)O)O)O)O)O)O
Standard InChIKey REBRERQNUHGTMS-PCGJYRBUSA-N
Standard InChI InChI=1S/C22H22O11/c23-13-8-12(9-14(24)17(13)26)21(30)33-22-20(29)19(28)18(27)15(32-22)10-31-16(25)7-6-11-4-2-1-3-5-11/h1-9,15,18-20,22-24,26-29H,10H2/b7-6+/t15-,18-,19+,20-,22+/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of 1-O-galloyl-6-O-cinnamoylglucose

The rhizomas of Rheum palmatum

Protocol of 1-O-galloyl-6-O-cinnamoylglucose

Structure Identification
Journal of Liquid Chromatography, 2014, 37(17):2546-2557.

Isolation and purification of seven compounds from extract of Rheum Palmatum L. by high speed counter current chromatography and rapid preparative chromatography[Reference: WebLink]

High speed counter current chromatography (HSCCC) combined with rapid preparative chromatography (RPC) was developed for the separation and purification of seven compounds from Rheum palmatum L. in this paper.
METHODS AND RESULTS:
Compounds dimmer-catechin, catechin, trans-3,5,4′-trihydroxystilbene-4′-O-β-D-(6′-O-gallayl)-glucoside, 1-O-galloyl-6-O-cinnamoylglucose, 1-O-Galloyl-2-O-cinnamoyl-glucose, rhein and emodin were isolated and purified by HSCCC using an optimized two-phase solvent system composed of n-hexane–ethyl acetate–n-butanol–water (1:2:1:4, v/v/v/v) and RPC. The purities of compounds 1, 3, 4 and 6 from HSCCC separation were over 98.70%, 96.75%, 98.20% and 98.07%, and those of compounds 1, 2, 4, 5 and 7 from RPC separation were 95.33%, 89.40%, 93.7%, 92.89% and 94.76%, determined by HPLC. The HSCCC and RPC fractions were analyzed by HPLC and electrospray ion source mass spectroscopy (ESI-MSn) in negative ion mode. The identification of the seven compounds from the extract of R. palmatum L. was based on matching their retention time, the detection of the molecular ions and the fragment ions of the molecular ion obtained in the MSn experiments with those of the data reported in the literature.
CONCLUSIONS:
The results demonstrated that HSCCC and RPC are feasible and efficient techniques for systematic isolation of bioactive components from R. palmatum L.

1-O-galloyl-6-O-cinnamoylglucose Dilution Calculator

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1-O-galloyl-6-O-cinnamoylglucose Molarity Calculator

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Preparing Stock Solutions of 1-O-galloyl-6-O-cinnamoylglucose

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 2.1626 mL 10.8131 mL 21.6263 mL 43.2526 mL 54.0657 mL
5 mM 0.4325 mL 2.1626 mL 4.3253 mL 8.6505 mL 10.8131 mL
10 mM 0.2163 mL 1.0813 mL 2.1626 mL 4.3253 mL 5.4066 mL
50 mM 0.0433 mL 0.2163 mL 0.4325 mL 0.8651 mL 1.0813 mL
100 mM 0.0216 mL 0.1081 mL 0.2163 mL 0.4325 mL 0.5407 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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