Isopropyl ferulate

CAS# 59831-94-6

Isopropyl ferulate

Catalog No. BCN8686----Order now to get a substantial discount!

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Isopropyl ferulate: 5mg Please Inquire In Stock
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Quality Control of Isopropyl ferulate

Number of papers citing our products

Chemical structure

Isopropyl ferulate

3D structure

Chemical Properties of Isopropyl ferulate

Cas No. 59831-94-6 SDF Download SDF
PubChem ID 6434600 Appearance Powder
Formula C13H16O4 M.Wt 236.26
Type of Compound Phenylpropanoids Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name propan-2-yl (E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoate
SMILES CC(C)OC(=O)C=CC1=CC(=C(C=C1)O)OC
Standard InChIKey KBTWMQRNUHIETA-FNORWQNLSA-N
Standard InChI InChI=1S/C13H16O4/c1-9(2)17-13(15)7-5-10-4-6-11(14)12(8-10)16-3/h4-9,14H,1-3H3/b7-5+
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of Isopropyl ferulate

The herbs of Ligusticum chuanxiong Hort.

Biological Activity of Isopropyl ferulate

In vitro

Synthesis of isopropyl ferulate using silica-immobilized lipase in an organic medium.[Pubmed: 21603272]

Enzyme Res. 2011;2011:718949.

Immobilization of lipases has proved to be a useful technique for improving an enzyme's activity in organic solvents.
METHODS AND RESULTS:
In the present study, the performance of a silica-immobilized lipase was evaluated for the synthesis of Isopropyl ferulate in DMSO. The biocatalyst was cross-linked onto the matrix with 1% glutaraldehyde. The effects of various parameters, molar ratio of ferulic acid to isopropyl alcohol (25 mM : 100 mM), concentration of biocatalyst (2.5-20 mg/mL), molecular sieves (25-250 mg/mL), and various salt ions, were studied consecutively as a function of percent esterification. Immobilized lipase at 25 mg/mL showed maximum esterification (~84%) of ferulic acid and isopropanol at a molar ratio of 25 mM : 100 mM, respectively, in DMSO at 45°C in 3 h under shaking (150 rpm).
CONCLUSIONS:
To overcome the inhibitory effect of water (a byproduct) if any, in the reaction mixture, molecular sieves (3 Å × 1.5 mm; 100 mg/mL) were added to the reaction mixture to promote the forward reaction. Salt ions like Ca(2+), Cd(2+), and Fe(2+) enhanced the activity of immobilized biocatalyst while a few ions like Co(2+), Zn(2+), Mg(2+), Mn(2+), Al(3+), and Na(+) had mild inhibitory effect. Approximately, one third of total decrease in the esterification efficacy was observed after the 5th repetitive cycle of esterification.

Isopropyl ferulate Dilution Calculator

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Isopropyl ferulate Molarity Calculator

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Preparing Stock Solutions of Isopropyl ferulate

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 4.2326 mL 21.1631 mL 42.3263 mL 84.6525 mL 105.8156 mL
5 mM 0.8465 mL 4.2326 mL 8.4653 mL 16.9305 mL 21.1631 mL
10 mM 0.4233 mL 2.1163 mL 4.2326 mL 8.4653 mL 10.5816 mL
50 mM 0.0847 mL 0.4233 mL 0.8465 mL 1.6931 mL 2.1163 mL
100 mM 0.0423 mL 0.2116 mL 0.4233 mL 0.8465 mL 1.0582 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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References on Isopropyl ferulate

Synthesis of isopropyl ferulate using silica-immobilized lipase in an organic medium.[Pubmed:21603272]

Enzyme Res. 2011;2011:718949.

Immobilization of lipases has proved to be a useful technique for improving an enzyme's activity in organic solvents. In the present study, the performance of a silica-immobilized lipase was evaluated for the synthesis of Isopropyl ferulate in DMSO. The biocatalyst was cross-linked onto the matrix with 1% glutaraldehyde. The effects of various parameters, molar ratio of ferulic acid to isopropyl alcohol (25 mM : 100 mM), concentration of biocatalyst (2.5-20 mg/mL), molecular sieves (25-250 mg/mL), and various salt ions, were studied consecutively as a function of percent esterification. Immobilized lipase at 25 mg/mL showed maximum esterification (~84%) of ferulic acid and isopropanol at a molar ratio of 25 mM : 100 mM, respectively, in DMSO at 45 degrees C in 3 h under shaking (150 rpm). To overcome the inhibitory effect of water (a byproduct) if any, in the reaction mixture, molecular sieves (3 A x 1.5 mm; 100 mg/mL) were added to the reaction mixture to promote the forward reaction. Salt ions like Ca(2+), Cd(2+), and Fe(2+) enhanced the activity of immobilized biocatalyst while a few ions like Co(2+), Zn(2+), Mg(2+), Mn(2+), Al(3+), and Na(+) had mild inhibitory effect. Approximately, one third of total decrease in the esterification efficacy was observed after the 5th repetitive cycle of esterification.

Description

Isopropyl ferulate, isolated from Rhizoma et Radix Notopterygii (Qianghuo), is used in the reduction of pharmaceuticals, preparation of antifungal agents, cosmetics and as antioxidant agent and so forth.

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