7-Methoxy-1-naphthylacetonitrileCAS# 138113-08-3 |
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| Cas No. | 138113-08-3 | SDF | Download SDF |
| PubChem ID | 11264068 | Appearance | Cryst. |
| Formula | C13H11NO | M.Wt | 197.23 |
| Type of Compound | Miscellaneous | Storage | Desiccate at -20°C |
| Solubility | Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc. | ||
| Chemical Name | 2-(7-methoxynaphthalen-1-yl)acetonitrile | ||
| SMILES | COC1=CC2=C(C=CC=C2CC#N)C=C1 | ||
| Standard InChIKey | PYJMGUQHJINLLD-UHFFFAOYSA-N | ||
| General tips | For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months. We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months. Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it. |
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| About Packaging | 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial. 2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial. 3. Try to avoid loss or contamination during the experiment. |
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| Shipping Condition | Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request. | ||
| Description | 1. 7-Methoxy-1-naphthyl-acetonitrile is an important intermediate in the preparation of anti-depression drugs. |
7-Methoxy-1-naphthylacetonitrile Dilution Calculator
7-Methoxy-1-naphthylacetonitrile Molarity Calculator
| 1 mg | 5 mg | 10 mg | 20 mg | 25 mg | |
| 1 mM | 5.0702 mL | 25.3511 mL | 50.7022 mL | 101.4045 mL | 126.7556 mL |
| 5 mM | 1.014 mL | 5.0702 mL | 10.1404 mL | 20.2809 mL | 25.3511 mL |
| 10 mM | 0.507 mL | 2.5351 mL | 5.0702 mL | 10.1404 mL | 12.6756 mL |
| 50 mM | 0.1014 mL | 0.507 mL | 1.014 mL | 2.0281 mL | 2.5351 mL |
| 100 mM | 0.0507 mL | 0.2535 mL | 0.507 mL | 1.014 mL | 1.2676 mL |
| * Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations. | |||||
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HPLC Determination of a Pharmaceutical Intermediate 7-Methoxy-1-naphthyl-Acetonitrile
Physical Testing & Chemical Analysis, 2009 , 45 (6) :654-5.
HPLC was applied to the determination of 7-Methoxy-1-naphthylacetonitrile(MONAN),which is an important intermediate in the preparation of anti-depression drugs.The Diamonsil C18 chromatographic column(250 mm×4.6 mm,5 μm) was used as stationary phase for separation of MONAN from co-existing by-products and impurities at column temperature of 20 ℃.A mixture of methanol and H2O(80+20) was used as mobile phase with flow-rate of 0.8 mL·min-1.UV-detection was made at the wavelength of 231 nm.Volume of sample solution introduction was 20 μL.Linear relationship between values of peak area and mass concentration of MONAN was obtained in the range of 2-48 mg·L-1.Detection limit(3S/N) found for the method was 105 μg·L-1.Precision and recovery were tested at the concentration level of 40.0 mg·L-1 of MONAN for 6 determinations,value of RSD and average recovery found were 0.034% and 99.7% respectively.
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