Valeroidine

CAS# 490-96-0

Valeroidine

Catalog No. BCN1920----Order now to get a substantial discount!

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Quality Control of Valeroidine

Number of papers citing our products

Chemical structure

Valeroidine

3D structure

Chemical Properties of Valeroidine

Cas No. 490-96-0 SDF Download SDF
PubChem ID 443012 Appearance Powder
Formula C13H23NO3 M.Wt 241.33
Type of Compound Alkaloids Storage Desiccate at -20°C
Solubility Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
Chemical Name [(3R,6R)-6-hydroxy-8-methyl-8-azabicyclo[3.2.1]octan-3-yl] 3-methylbutanoate
SMILES CC(C)CC(=O)OC1CC2CC(C(C1)N2C)O
Standard InChIKey APLLVFVOTXZBFO-RUJICJSRSA-N
Standard InChI InChI=1S/C13H23NO3/c1-8(2)4-13(16)17-10-5-9-6-12(15)11(7-10)14(9)3/h8-12,15H,4-7H2,1-3H3/t9?,10-,11?,12-/m1/s1
General tips For obtaining a higher solubility , please warm the tube at 37 ℃ and shake it in the ultrasonic bath for a while.Stock solution can be stored below -20℃ for several months.
We recommend that you prepare and use the solution on the same day. However, if the test schedule requires, the stock solutions can be prepared in advance, and the stock solution must be sealed and stored below -20℃. In general, the stock solution can be kept for several months.
Before use, we recommend that you leave the vial at room temperature for at least an hour before opening it.
About Packaging 1. The packaging of the product may be reversed during transportation, cause the high purity compounds to adhere to the neck or cap of the vial.Take the vail out of its packaging and shake gently until the compounds fall to the bottom of the vial.
2. For liquid products, please centrifuge at 500xg to gather the liquid to the bottom of the vial.
3. Try to avoid loss or contamination during the experiment.
Shipping Condition Packaging according to customer requirements(5mg, 10mg, 20mg and more). Ship via FedEx, DHL, UPS, EMS or other couriers with RT, or blue ice upon request.

Source of Valeroidine

The herbs of Atropa belladonna L.

Protocol of Valeroidine

Structure Identification
Science China-Chemistry, 2013, 57(2):252-264.

A novel and versatile method for the enantioselective syntheses of tropane alkaloids.[Reference: WebLink]


METHODS AND RESULTS:
A full account of the novel and flexible approach to hydroxylated 8-azabicyclo[3,2,1]octan-3-ones and 9-azabicyclo[3,3,1] nonan-3-ones is presented. Using keto-lactams as the starting materials, this two-step method consists of silyl enol ether formation with TBDMSOTf, lactam activation with Tf2O/DTBMP, and halide-promoted cyclization. Radical dechlorination of the resulting 1-halotropan-3-ones led to the corresponding hydroxylated tropan-3-ones, which can be hydrogenated to yield 3α,6β-dihydroxytropanes.
CONCLUSIONS:
Starting from optically active keto-lactams, the method has been applied to the enantioselective syntheses of (+)-(1S,3S,5R,6S)-pervilleine C (6), (+)-(1S,3R,5S,6R)-Valeroidine (3), (+)-(1S,3S,5R,6S)-dibenzoyloxytropane (8), and (+)-(1S,3S,5R,6S)-merredissine (9).

Valeroidine Dilution Calculator

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Valeroidine Molarity Calculator

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Preparing Stock Solutions of Valeroidine

1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 4.1437 mL 20.7185 mL 41.437 mL 82.8741 mL 103.5926 mL
5 mM 0.8287 mL 4.1437 mL 8.2874 mL 16.5748 mL 20.7185 mL
10 mM 0.4144 mL 2.0719 mL 4.1437 mL 8.2874 mL 10.3593 mL
50 mM 0.0829 mL 0.4144 mL 0.8287 mL 1.6575 mL 2.0719 mL
100 mM 0.0414 mL 0.2072 mL 0.4144 mL 0.8287 mL 1.0359 mL
* Note: If you are in the process of experiment, it's necessary to make the dilution ratios of the samples. The dilution data above is only for reference. Normally, it's can get a better solubility within lower of Concentrations.

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